(E)-2,4-Dichloro-6-{1-[(2-chloroethyl)imino]ethyl}phenol
نویسندگان
چکیده
منابع مشابه
(E)-2,4-Dichloro-6-{1-[(2-chloroethyl)imino]ethyl}phenol
The title Schiff base compound, C(10)H(10)Cl(3)NO, was prepared by the condensation of 1-(3,5-dichloro-2-hy-droxy-phen-yl)ethanone with chloro-ethyl-amine. The imine adopts an E configuration with respect to the C=N bond. The H atom of the phenolic OH group is disordered over two positions with site occupation factors of 0.52 (7) and 0.48 (7), respectively, and the major occupancy component is ...
متن کامل(E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
The title Schiff base compound, C(13)H(8)Cl(3)N(3)O(2), was synthesized by the condensation reaction of 3,5-dichloro-salicyl-aldehyde with 6-chloro-nicotinic acid hydrazide in 95% ethanol. The mol-ecule is nearly planar, with a dihedral angle of 1.9 (2)° between the aromatic ring planes, and an intra-molecular O-H⋯N hydrogen bond is observed. In the crystal, the mol-ecules are connected by inte...
متن کامل4,6-Dichloro-2-[(E)-(2-{[(E)-3,5-dichloro-2-oxidobenzylidene]azaniumyl}ethyl)iminiumylmethyl]phenolate
The asymmetric unit of the title compound, C(16)H(12)Cl(4)N(2)O(2), comprises half of a potentially tetra-dentate Schiff base ligand, located about a twofold rotation axis which bis-ects the central C-C bond of the ethane-1,2-diamine group. In the solid state, the compound exists in the zwitterionic form. There are two intra-molecular N-H⋯O hydrogen bonds making S(6) ring motifs. In the crystal...
متن کامل4,6-Dichloro-2-((E)-{4-[(E)-3,5-dichloro-2-hydroxybenzylideneamino]butylimino}methyl)phenol
The asymmetric unit of the title compound, C(18)H(16)Cl(4)N(2)O(2), comprises half of a potentially tetra-dentate Schiff base ligand. It is located about a twofold rotation axis that bis-ects the central C-C bond of the butane-1,4-diamine group. There are two intra-molecular O-H⋯N hydrogen bonds making S(6) ring motifs. In the crystal, mol-ecules are linked by pairs of weak C-H⋯Cl inter-actions...
متن کامل4,6-Dichloro-2-{[(E)-(3-{[(E)-3,5-dichloro-2-hydroxybenzylidene]amino}-2,2-dimethylpropyl)imino]methyl}phenol
In the title compound, C(19)H(18)Cl(4)N(2)O(2), a potential tetra-dentate Schiff base ligand, the dihedral angle between the two benzene rings is 48.01 (10)°. The configuration about the two C=N bonds is E and two intra-molecular O-H⋯N hydrogen bonds make S(6) ring motifs. In the crystal, mol-ecules are linked along the b axis via inter-molecular C-H⋯Cl inter-actions. The crystal structure is f...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2010
ISSN: 1600-5368
DOI: 10.1107/s160053681004448x